The solvent was evaporated to dryne

The solvent was evaporated to dryness and the obtained residue triturated with n-hexane. The obtained solid was collected by filtration and crystallized from ethanol/n-hexane to give the prod-ucts 3d and 3g as identified by melting point and TLC in comparison with samples prepared according to proce-dure B.

結果 (中文) 1:

溶剂都蒸发干燥和脱粒机与 n-己烷所得的残渣。所得的固体是收集的过滤和结晶从乙醇/n-己烷给乾豪 3d 和 3 g 与样品准备为切入 B.根据确定的熔点和薄层色谱法

結果 (中文) 2:

蒸干溶剂，将得到的残余物用正 - 己烷研制。得到的固体通过过滤收集，并从乙醇/正己烷中结晶，得到督促-UCTS三维和3G中的样品进行比较确定的熔点和TLC根据PROCE-杜热B.制备

結果 (中文) 3:

溶剂蒸发干燥，得到的正己烷残留研究。得到的固体通过过滤收集结晶乙醇/正己烷给产品3D和3G的熔点和TLC鉴定按照程序B.制备样品的比较