Compound 2 (1 mmol) added to CH2Cl2

Compound 2 (1 mmol) added to CH2Cl2 (15 mL) was stirred at
0 C and oxalyl chloride (1.5 mmol) was dripped into the mixture
and stirred at room temperature for 6 h. After the reaction, the
solvent and excess oxalyl chloride was evaporated under reduced
pressure. Toluene (15 mL) and KSCN (1.2 mmol) were added to the

結果 (中文) 1:

复方 2 (1 毫摩尔) 添加到 CH2Cl2 (15 毫升) 在搅拌0 C 和草酰氯 (1.5 毫摩尔) 滴入混合物和搅拌在室温下 6 h。反应完成后，溶剂和过剩的草酰氯蒸发下减少压力。甲苯 (15 毫升) 和氰酸 (1.2 毫摩尔) 被添加到

結果 (中文) 3:

化合物2（1毫摩尔）加入二氯甲烷（15毫升）搅拌在
0  C和草酰氯（1.5毫摩尔）滴入混合
和在室温下搅拌6小时，反应结束后的
溶剂和多余的草酰氯下蒸发压力降低
。甲苯（15毫升）和硫氰酸钾（1.2毫摩尔）添加到